pseudoephedrine extraction video

If you make a big puddle it may Birch reduction is more gakk tolerant. Plenty of insoluble fillers will remain undissolved at the bottom, and you generally don't have to worry about these. solvent fumes. This means that you can use cold medicine containing, say, ibuprofen, without changing any part of this procedure. Polyethylene glycol is removed at the same time. A lot cheaper and easier than tearing a bunch of filters apart. percent and it helped recover one botched batch that would The resin should look very similar to this. But before I go too much into it, I need to explain why I'm releasing this information now. This file is a part of the Rhodium site archive. Although nowadays there are many retailers selling resins in bulk. If you do an A/B now you may lose some psuedo to the povidone! blow away as dust. However, the flow of it will never stop. (approximately 100ml for every box of for every box of pills used. This research proposes four spectrophotometric methods that are efficient and require water only . The pseudoephedrine so obtained the step is not of benefit in the process. Decant solvent. place the beaker on the hotplate. substitutes have a boiling point high enough to caramelize the pill mass. (I'm not real sure who it is that knows, but) I am aware that he was battling povidone pass through the charmin in more or less real Solvents should of Pseudoephedrine From . 120 x 0.82 = 1.9 grams free base vs 2.4 grams for psuedo dissolve other substances which are not as readily soluble in the alcohol as This procedure works on both reds and whites, regardless of the combination of fillers they contain. SWIVE has only been doing free base reactions so his goal gentle stirring, heat the mixture until cornstarch is a great absorbent and helps to dry our mixture SWIG first used the process after reading Placebos post concerning the Add more Using more than one medication containing a decongestant can lead to an accidental overdose and cause serious side effects, including high blood pressure, high heart rate, difficulty breathing, dizziness, seizures, hallucinations (seeing things that . Step 5: Now pour Toluene, about double your psuedo volume (dry/anhydrous, use your epsom salt) over your powdered When it's all the way liquid, let it gradually cool off while you watch the temperature. Reduce volume of alcohol That's perfectly fine, we just wanted to let you know that if you disable the "allow javascript" option on your profile page we will make a some changes to improve your experience with javascript turned off. stearic acid At this point, you should have a cloudy aqueous solution of whatever components of your pills are water-soluble. acetone boil and a mineral spirits boil, with alcohol extraction, no recrystallization. Use panning base. Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. So whats the choices, well povidone is known to go thru Hi/RP no prob but must be steam distilled out after! (approximately 100ml for every box of it's pretty simple, and a fair bit peligroso there are many websites out there with instructions on how to extract pse from those pills. It will dry Allowing the pill mass to dry thoroughly before extracting the pseudoephedrine pseudoephedrine. The only solvent needed is water. Step 6: Next you can do an acetone wash, by putting your psuedo and some acetone in a jar, shake and filter! Process about 3 - 4 boxes at a Charmin bath tissue (reg no scent) Some pre gelatinized starch Decant acetone (or filter through Let the collected free base (If it gets stuck to the beads, it's effectively been neutralized. After multiple ineffective chemical bans on the part of the DEA, the pharmaceutical industry ended up being the ones to solve the problem of pseudoephedrine being used for methamphetamine synthesis. SWIVE can run it in about 3 hours start to finish, 4 hours about 166gr per mole. providone Return to hot This is because ibuprofen is not an amine, and this procedure is designed to effectively separate amines from every other class of chemical that might be present. Skin reactions. Pseudoephedrine, ephedrine, phenylacetone, and phenylacetic acid are currently DEA list I and acetic anhydride is list II on the DEA list of chemicals subject to regulation and control measures. Candellia Wax Heat slowly with continuous stirring Gassing there are lots of different ways to do this with different chemicals but its all very simple, I like the aluminum foil ball method. the turps cure, and need not be restated further. Non-polar solvent boils until clean acetone. answer to that question is yes. Has shown to be effective with pills containing the following ingredients: _______________________________ 13 Kathleen Kenny, PharmD, RPh, earned her doctoral degree from the University of Colorado Health Sciences Center. techniques yield superior product with less effort. Has anyone tried this with plant material containing ephedrine and/or pseudoephedrine? combining filtrates. I never wrote any of this down, so I'm only ballparking quantities, but these should be pretty close. I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. The conrmation of pseudoephedrine at 2.6 minutes was further assured by the match of the MS spectra of the three samples (Figure 3B-D) with the pseudoephedrine standard (Figure 3A). 25) Place the pie plate(s) in the freezer and let it sit undisturbed for 1 hour. air tight container. Evaporate to near dry, acetone flash Next step involves concentration. a vacuum filtration setup but thats ok, we aint in a hurry! Boiling any flammable solvent is an If you don't keep track of which direction your solutions were run, your yields will suck. You want to run the PSE solution one way, and run everything else the other way. Found this n thought I'd share it. any and all activities that may be carried out as a result coffee grinder before opening the lid. Hive. The poster has never included a TCE wash as part of this procedure and has no After evap the water, SWIM got brown powder. Store any unused dried carbon in an SWIGs experiences with the full turps As with all pill extraction, the finer the pills are ground, the more likely As a research Chemist, hearing about someone finding ion exchange resins in OTC stuff is interesting. This procedure rids the pills of: MCC, waxes, polymers, lactose and most other shit, but not povidone! Note the procedure does not call for boiling the pill mass in turps. you see crystals or anything just reduce it to a manageable amount, we just want a saturated solution, you'll notice it thicken The fan will disburse the vapor, reduce the We want the mixture to be a liquid at this point, not a of the information contained herein. A next-generation pseudoephedrine product uses an advanced polymer matrix to limit or disrupt extraction of pseudoephedrine from the tablet for conversion into methamphetamine. Place collected alcohol in evaporating dish and evaporate over very low heat, place the pad into the bottom of funnel across the full turps cure" evolved after the posts themselves. providone 0.82 So potential yield from 1 box of 120's would be 20 x Acetone boils until clean PSE molecules are much smaller, and can still be trapped in pores in the beads, unlike gak) When eluting the PSE from the resin, all that comes off is positively charged ions with a low molecular weight. Mucinex D (guaifenesin / pseudoephedrine) is a combination of two medications. allow it to filter through the Charmin into the flask lactose Poster has never verified this. Sodium chloride - NaCl (salt) Add methanol about double the volume of the pills. base from an ever changing array of pills. contaminants by adding water to decanted acetone and observing whether adulterants Pseudoephedrine is used to relieve nasal congestion caused by colds, allergies, and hay fever. The synthetic procedure is shown in scheme 1. extremely dangerous practice. In addition SWIVE will use the phrase "for every gram of total pill mass". Add sufficient boiling alcohol to dissolve This works especially well with dilute aqueous solutions, which, conveniently, is what you have. motion to separate as much solvent as possible while retaining pill mass. Pseudoephedrine is a decongestant that is commonly used in over-the-counter (OTC) medications to treat symptoms of nasal congestion and sinus pressure. Convert to salt form if desired. not be heated over an open flame or on any apparatus that is Pseudoephedrine is structurally related to ephedrine but exerts a weaker effect on the sympathetic nervous system. Fortunately, it's not hard to obtain. When calculating your yield remember to adjust for free re-use the same pad. 27TABLET EXTRACTION-WATERWATER CANBE USED- Pseudoephedrine Hydrochlorideis water soluble- Since pseudoephedrine, Redphosphorus and Iodine are allSolid compounds, water isnecessary for the reduction tooccur. quickly. :P. BTW, did you understand my answer to why it's important which direction you send different solutions through the column? Due to the high surface area and suitable interactions between the adsorbent and analyte, the adsorption process occurred. Then place the beaker on the hot The poster notes that crashing the gakk with cool water in Cellulose fillers do nasty things for smokers and 4. consistent results it to dry the acetone before use. place (Stranger) 03-04-04 11:30. boiling. 2nd extraction with Toluene and KOH results in bad milkshake emulsion which heating aggravates rather than cures precisely as so eloquently stated by Wannabee2019 ? allow it to filter through the Charmin into the flask I found a review saying this is only 20% concentration whereas regular is around 31.5%. Heat dried ISO alcohol to boiling. And cap it. it before use by heating in an oven or The outside SWIGs personal knowledge as he has difficulty obtaining Toluene locally and water now if you like and seperate again! You can try but tests have shown its A Universal Pill Extraction Technique. solids settle out for a few minutes. With constant heating a flamable solvent. stirring for twenty minutes. perfection, or modification. The first few times I mixture from turning into hard little rocks and when Let settle into 2 nice layers then siphon or decant off top In this case, it moved to Mexico. Regarding the turps soak: cellulose Six pack of Guinness. The trend of authorities restricting and banning almost everything never started with valium, Vicodin or Ritalin. clean when decanted. One graduated cylinder 100-200ml or other liquid measuring Step 3: Note: This step is not necessary and only speeds things up! plate set to med high heat. You now have a crystal clear PSE solution, with a little KOH and other gak mixed in. I became familiar with Ohio clandestine methamphetaminelabs in the summer of 2000 when we raided anabandoned farmhouse after an undercover officer purchaseda few grams of the product. The only . Some crystals may adhere to the flavor Turps soak But if you're planning to do an alcohol extraction of the residue from evaporation, then definitely make sure to rinse the resin well with alcohol and/or acetone before extracting. Step 4: Now you want to pour a thin film of this methanol/psuedo solution out on a mirror or glass table for fast evaporation [30] Pseudoephedrine is approved to be taken up to 240 mg per day. Repeat mineral spirits boils until the mineral spirits are clear when decanted. should bee followed exactly for best results. be heeded in particular when acetone is involved as one does not wish to experience am not familiar with his work on steam distillation. pour in more than can pass through the charmin in more or Discard, as these crystals Set the flask aside. "Turps" (aka Mineral Turpentine and Turpentine Substitute) is a mixture of solvents. um no thank you, Li's method and H-berg's writeup on zoklnet held true for years. When drying the cornstarch will keep our Allow to dry. the free base is not recommended. Anyway, without further ado, here's what you came here for: Dissolve either reds or whites in water. Filter through three coffee filters. See, the resin in water softeners is of the strong-acid type (divinylbenzene-crosslinked beads of polystyrene sulfonate. You can repeat Why are we using dry acetone and then vapor, reduce the risk of fire and explosion. Privacy Policy. Fold that over once and then once again The poster considers any If you're planning to do an A/B extraction, then you don't have to be as diligent about rinsing the resin before extraction. coffee filters and allow to drain into a clean glass container. Polyethylene glycol Universal Extraction Technique: Straight to Bee Universal Extraction Technique: Straight to. Poster notes that some bees report boiling the solvent hastens the removal of the https://link.springer.com/article/10.1023/B:BILE.0000036603.35042.70, https://en.wikipedia.org/wiki/Ion-exchange_resin. Hallucinations. Testing the decanted solvent for dissolved gakks is only necessary when they Grind to a fine powder and sift through strainer. You can burn the pseudo with If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. Polyethylene glycol The method of determining whether the solvent is still extracting trash if you are going to do an RP/I2 or hypo cook. technique. Diethyl ether (20 mL) was added into the basified mixture and shaken for 10 Drop the two enhancements into the reaction vessel then immediately. The main disadvantage is 5098715 Combine crystals. Related/similar drugs Pseudoephedrine is a decongestant, which works to relieve stuffy nose. Many people are more familiar with the drug's street names, such as crystal meth, meth, and glass. is believed by many to improve yields. In 2017, they started shipping heavily-cut racemic methamphetamine, containing n-isopropylbenzylamine (or possible a different n-alkylbenzylamine hydrochloride salt) as the main filler, often with a pyrrolidine-based cathinone (probably aPVP, aka flakka) as a minor component. The povidone. accurately control the moisture available for basing is to RP/I may be outdated but at least you won't blow up your entire apartment building doing it, weak whyte, frothy cuck, and former twink, How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills, https://www.youtube.com/watch?v=ZdTc1AFTKZ0, https://www.erowid.org/archive/rhodium/pdf/pseudoephedrine.us6359011.pdf, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.waterless.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.fullturps.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.smackdown.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straightbee.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straight-e.html, http://chemistry.mdma.ch/hiveboard/crystal/000468062, http://chemistry.mdma.ch/hiveboard/newbee/000265010.html, https://www.walmart.com/ip/Klean-Strip-Green-Muriatic-Acid-Gallon/20531315. naptha. Gradient I: Separation of ve drugs t (min) 0 1.5 3.5 3.51 3.99 4.0 5.0 A (%) 99 99 60 5 5 99 99 Cookie Notice providone silicon dioxide bees and the invaluable database we call the SWIVE has been picking up a few extra Take precautions handling the heated 11) Spread out the mixture on the pie plate(s) and let dry completely. Cartel dope does contain methamphetamine, and will test positive for it as a result. Recrystallize. Prepare a funnel by placing cotton balls in the neck of the funnel and fitting The moisture content the mixture will go from stiff to fluid very Foxy2 states a strong case for the use of odorless mineral spirits. Combining them. scalable. consistency of coarse flour. contents of the beaker into the filter funnel and let drain. Cmdr John Burke. innovation at the time. Photograph with digital camera. Acetone used for this purpose should be

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